Thorshammer
Member
My online grammar is terrible. I'm fully aware. I keep saying I'll work on it, but I am taking way more interesting classes and don't get the same dopamine fuel that overrides my ADD.
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Thanks.
Ghoul
Member
It’s all good brother, couldn’t help myself
I appreciate your intelligent skepticism.
While I appreciate Jano, his service to the community has been substantial, transformative even, he’s also a vendor who does this primarily to make money. Like every vendor there should always be some healthy questioning and pressure applied. It’s in everyone’s best interest, and he is responsive to his customer base, expanding tests and refining his methods over the years. He’s a humble guy, and never denies the limitations of his testing, but the “halo effect” defensively conferred on him by some who act like he’s a Nobel biochemist gracing us with his presence and shouldn’t be questioned isn’t helpful.
I do respect his reports.It’s all good brother, couldn’t help myself
I appreciate your intelligent skepticism.
While I appreciate Jano, his service to the community has been substantial, transformative even, he’s also a vendor who does this primarily to make money. Like every vendor there should always be some healthy questioning and pressure applied. It’s in everyone’s best interest, and he is responsive to his customer base, expanding tests and refining his methods over the years. He’s a humble guy, and never denies the limitations of his testing, but the “halo effect” defensively conferred on him by some who act like he’s a Nobel biochemist gracing us with his presence and shouldn’t be questioned isn’t helpful.
Thorshammer
Member
All good helps me improve I'm not sensitive if I'm wrong. And Jano has made a huge positive impact for the community. I remember before he was around Chinese GH was a joke and testing has forced dramatic improvement in that regard. I switched to AB because I had emailed Jano multiple times with zero response for months. If there is substantial difference I don't mind the huge price difference but I'm not just gonna go off fan boy rumors I think I will send him and AB some identical samples that I have already done UV VIS analysis on and see what kind of variations I get.It’s all good brother, couldn’t help myself
I appreciate your intelligent skepticism.
While I appreciate Jano, his service to the community has been substantial, transformative even, he’s also a vendor who does this primarily to make money. Like every vendor there should always be some healthy questioning and pressure applied. It’s in everyone’s best interest, and he is responsive to his customer base, expanding tests and refining his methods over the years. He’s a humble guy, and never denies the limitations of his testing, but the “halo effect” defensively conferred on him by some who act like he’s a Nobel biochemist gracing us with his presence and shouldn’t be questioned isn’t helpful.
Thorshammer
Member
Good stuff. Not sure why my ability to react to comments is disabled in this post.
You don't get reaction options for the UG until about 200 posts / reaction score IIRC.
xrayphoton13
Member
Exactly. I've seen several concerning errors his team has made. They're far from perfect. Hopefully these growing pains get sorted outIt’s all good brother, couldn’t help myself
I appreciate your intelligent skepticism.
While I appreciate Jano, his service to the community has been substantial, transformative even, he’s also a vendor who does this primarily to make money. Like every vendor there should always be some healthy questioning and pressure applied. It’s in everyone’s best interest, and he is responsive to his customer base, expanding tests and refining his methods over the years. He’s a humble guy, and never denies the limitations of his testing, but the “halo effect” defensively conferred on him by some who act like he’s a Nobel biochemist gracing us with his presence and shouldn’t be questioned isn’t helpful.
Thorshammer
Member
analytical chemistry isn't perfect brother. Thats why I was questioning the criticism of other labs on small margins considered normal deviations. From the balance to volumetric glass and pipettes used for dilutions to the colums in the tower and detector and comparisons to calibration curves and standards expecting exact calculations is like asking for magic. People forget the limitations of these techniques or the complexity involved.
Appreciate the input. Ignore the childish behavior of some members.
Luka.Halotestin
Member
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Thorshammer
Member
Ouch time to bust out the solvents and give that shit a bath.
Luka.Halotestin
Member
Luka.Halotestin
Member
Any suggestions?
Thorshammer
Member
Probably experiment with acetone or ethanol first for easier evaporation. You have access to a vacuum oven?
Thorshammer
Member
Start with small amounts. You need a way to check improvement each time. Record MP duration and make sure it keeps getting shorter . Obviously sending for HPLC during small trial runs isnt an option
Great thread although the subject matter is shared with cautionary note. Thanks again for meticulously capturing your work @mongo5165.
Buffering
New Member
Did you buy this garbage from aasraw?
Thorshammer
Member
weigh the sample in the dish you will recrystalize it in on your balance and keep it in that so you can record the final weight. So you know how much was lost and can calculate what was removed also
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