First batch

[Denver]

Recently had 3 vials of test cyp from a recent brew that Were temporarily put in the fridge over night. The next day the test looked like it had crashed. One of the vials was basically solid slush that was able to be thawed out. One of the vials was totally fine and the other one was somewhere between the totally clear vial and totally crashed vial. Brewing instructions were followed verbatim from the Quality Raw web site, but the powder did not come from there. Any idea what is going on here?

 

[Docd187123]

You had one vial crash, one vial somewhat crashed, and one vial that didn't crash.....

 

[Denver]

You had one vial crash, one vial somewhat crashed, and one vial that didn't crash.....

Yes. All made from the same batch.

 

[Docd187123]

Yes.

Well that's what went down. I'm not sure what more you're looking for?

 

[Denver]

Well that's what went down. I'm not sure what more you're looking for?

What would cause the difference between vials, since all the vials were from the same batch???

 

[Docd187123]

Could be different pressure or temps in the vials.

 

[Denver]

The non-crashed vial was filtered first while the test was the warmest and the totally crashed vial was the last and coolest (it was pushed thru a new filter), so maybe it was the temp. I didn't realize that would make a difference. Should it still be ok to use as long as I heat it up each time?

 

[Docd187123]

I meant temp as in the temp it was before putting in the fridge not filtering but a few degrees could make a difference yes.

It'll be fine. Once you heat it up once it should stay in solution if the recipe you used was good

 

[Denver]

I meant temp as in the temp it was before putting in the fridge not filtering but a few degrees could make a difference yes.

It'll be fine. Once you heat it up once it should stay in solution if the recipe you used was good

After I heated the crashed vial I left it at room temp and it went right back to the sludge.

 

[Docd187123]

After I heated the crashed vial I left it at room temp and it went right back to the sludge.

Bad recipe probably. What did you use?

 

[Denver]

Bad recipe probably. What did you use?[/QU
25g Test Cyp
2ml BA
10m BB
69.25 grape seed Oil
Heated everything to 160 degrees during melt and mix

 

[Docd187123]

What was the total volume you made?

 

[Denver]

What was the total volume you made?

100 ml

One other thing, the first vial was filtered as soon as the test turned to solution in the beaker in the hot water bath. I left the remaining solution in the hot water while filtering the first batch. Maybe the extra time in the hot water (half hour or so) was not good???

 

[Docd187123]

100 ml

You got exactly 100ml out of this? Measured it to verify? To me it seems like it would total closer to 105ml.

Anyway, it comes out to roughly 250mg/ml. Test Cyp has much lower solubility than enanthate so it's not uncommon for it to crash. You can either heat it up before each injection or try and add more solvent to the mix but that would also dilute your final concentration some.

 

[nophat]

10% bb ?
Take all the vials open them up and mix together.
Bring the bb up to 18%.
Like doc said bad recipe for cyp.
When you reheat it let the swirls leave stir it slowly and watch the swirls leave.

 

[Big_paul]

Test cyp you need 20% bb. Like Doc mentioned, it could be pressure, my guess is that's not the problem. Why did you put it in the fridge?

 

[Big_paul]

If they are identical, they would all react the same. Did you add bb separately to each vial? Its most likely solvents are at different levels.