Puzzling crash issue

Small batch consisting of three 10ml vials, gear (stanolone 50mg/ml) from from first vial filled remained in solution, second and third crashed big time at 24h mark.

What went wrong?
 
What where your solvents?

33% BB 2% BA

I was thinking that I must of somehow got different gear % in the vials maybe from the mixture not being homogeneous, maybe larger yet different particles sunk to the bottom before I draw from the becker.
 
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