Save your unusable raws Guaranteed.

[Photon]

After it crashes, I would remove as much ethanol as possible with a pipette or a syringe, this way any contamination remaining in the ethanol dosent make its way into the final product. Then evap the the remaining residual ethanol or water

I may have removed too much ethanol at step (3)

it's now turning into a complete block in my freezer.
20g in 50ml (total)
Should i add water?


There's something weird about this, it ended up leaving adhesive tape-like stains all over my beakers which im having a hard time removing. Hot water + soap + scrubbing doesn't remove it at all. The stains have the same strong chemical smell as the raws (which is a plus i guess).

 

[Photon]

There's something weird about this, it ended up leaving adhesive tape-like stains all over my beakers which im having a hard time removing. Hot water + soap + scrubbing doesn't remove it at all. The stains have the same strong chemical smell as the raws (which is a plus i guess).

Boiling water got rid of it lol

 

[mongo5165]

Boiling water got rid of it lol

Yeah it probably the testosterone with the impurities leaving the stain. Due to the high melting point its really difficult to remove. With test c, I had to use boiling water to clean it up. Acetone or IPA works well also.

If its cold, dont add water until you drain off the raws. If you add it to the ethanol, everything will just turn into a slushy or a block if ice. I just use the water rinse to clean the remaining solvent off before the vacuum chamber.

That's some serious contamination right there... if it dosent clean up, maybe do 2 re-x's, one with EA/heptane and ethanol on the second. This way you cover all bases for polar and non polar contamination

 

[Photon]

That's some serious contamination right there... if it dosent clean up, maybe do 2 re-x's, one with EA/heptane and ethanol on the second. This way you cover all bases for polar and non polar contamination

Its 86% TRE not test

 

[mongo5165]

Its 86% TRE not test

Ah okay my bad. Yeah the tren ace im working on had been a pain in the ass. Im gonna switch up the solvent group and see if that works better.

 

[dinfaralt]

Should i add water?

trenbolone & test is almost insoluble in water

i think you have added way too little ethanol

testo solubility in ethanol room temp 20-25c = 200mg/ml

trenbolone ace is 10mg/ml in 20-25c

testosterone in warm ethanol 60-78c is 300-400mg/ml

that would give us 1g testotserone per 5ml for room temp.

for trenbolone ace u would need alot of ethanol.

you could heat the ethanol(dangerous) to make the tren more soluble in it

the brother in here have recommened some better options for u already that is better for trenbolone solubility

Ethanol is not a good choice. It is way too polar. Ethyl acetate/heptane is best. Acetone/heptane second. IPA/heptane third. The EA/heptane is the cleanest. Ethanol will oil out. Also with TRE after filtration you most definitely want to concentrate down. Evap to 40-50%. TRE will use more heptane as well.

 

[Photon]

trenbolone ace is 10mg/ml in 20-25c

Right now i have it at 20g/50ml for TRE.
so 400mg/ml

it turned into a ice block but it does look pretty nice lol

Im at the crashing stage btw, started with 300ml and evap'd till 50ml before freezing.

 

[dinfaralt]

Right now i have it at 20g/50ml for TRE.
so 400mg/ml

it turned into a ice block but it does look pretty nice lol

i hope it works out, i believe the other solvents will clean it better. its unnecasary a pain the ass + less effective.

 

[Photon]

i hope it works out, i believe the other solvents will clean it better. its unnecasary a pain the ass + less effective.

It looks like it's full of crystals, but the ethanol lumped up with it.
I added water to it and stirred it.
Next step is water bath to wash out the ethanol.

 

[Photon]

I think i screwed up somewhere.
Should i dissolve it with ethanol again and recrash?
Adding water to dilute it might have been a mistake lol

I now have a solid block at the bottom which looks like this

@mongo5165

 

[IndividualMan]

Should i dissolve it with ethanol again and recrash?

yes.
you could also just grind it down and evap on low heat, that helps getting Ethanol out
Molecular sieves help getting moisture out, so you could/ should put thsoe in as well

 

[dinfaralt]

I think i screwed up somewhere.
Should i dissolve it with ethanol again and recrash?
Adding water to dilute it might have been a mistake lol

I now have a solid block at the bottom which looks like this

@mongo5165

View attachment 367973

its actually disgusting how much crap is in your tren vs the crystals you can see i geniuenly dont know if i should laugh or be disgusted people are injecting that

 

[Photon]

yes.
you could also just grind it down and evap on low heat, that helps getting Ethanol out
Molecular sieves help getting moisture out, so you could/ should put thsoe in as well

I think the issue was that i got too much ethanol out in the first place lol

I think it precipitated when i added water instead of crystalisted

 

[dinfaralt]

I think the issue was that i got too much ethanol out in the first place lol

I think it precipitated when i added water instead of crystalisted

hey atleast you're walter white of the steroid crystals next time around buddy

indian poop raws? no challenge for your greatness!

 

[Photon]

hey atleast you're walter white of the steroid crystals next time around buddy

indian poop raws? no challenge for your greatness!

Dissolving it again with ethanol again fixed it
20g @ 200ml total.

tiny snowflakes are forming