I followed your suggestion above and DHB stays in the solution completely at least for 15hours. The only mistake I made was that temp was around 275 for only a few minutes at the very beginning of the process and black snapoffs tops started to deform and I quickly took the vials out and removed the snapoffs. Because TGI fills the vials to the top (which we like!) and expansion of the liquid at hot temps, some oil leaked oil of vials. Then i set the temp back to 200, put the vials back in for about 1.5hours during which time I shook the vials vigorously every 10mins.
@Jrock83 ,
@bolder @Urgentfury12 ,
@TitaniumGear (TGI) , Do you guys think I should filter the oil given that the vials were at high temp of about 275 for a few minutes, in case particles from the rubber cap or plastic snapoffs leached in the solution?