Do you get much Insoluble crap that filters out once you dissolve it in ethanol?
MESO-Rx
Anabolic Steroids
Save your unusable raws Guaranteed.
- Thread starter TheScholarOfBrew
- Start date
Photon
Member
I do get some soot like particles at the bottom, which i assume is just dust.
It's not alot tho. Im using a PTFE .1um filter but im pretty sure those can be filtered out via a .45um given the size of it.
IndividualMan
Member
currently on my new cycle: 500 test E, 178mg Tren E, 22mg dust, soot and other shit, split into MWF injections.
Thorshammer
Member
Don't go straight from hot plate to freezer let it cool slowly, room temp then fridge then ice bath then freezer if you had good TRE you can seed it. You dont want it crashing to fast and oiling out because you just trap all the impurities back in the crystal lettuce.Threw my stinky TRE raws in ethanol
surprisingly easy to dissolve
20g/300ml and it dissolved with barely any heat
this is what im planning to do
(1) raws in ethanol
(2) hot ptfe filter .1um
(3) evap ethanol
(4) crash in freezer
(5) water bath
(6) evap till dry
anything im missing?
i do not want to use any other solvents
Took a picture before sealing it.
I can smell it 10 feet away.
Thorshammer
Member
Y
Ou will need to reduce the volume of that ethanol. I can't stress proper ventilation enough if not working in a fume hood.
Photon
Member
It's in my fridge now, q.s till 700ml with ethanol.
I created some crystals in the freezer then moved it over to the fridge.
I'm not sure if ill ever use it, I'm just gonna leave it there for the interim lol
I ended up buying oils from a vendor with 98% TRA
Thorshammer
Member
Thats a lot of ethanol and nit a lot of product most will remain soluble it has a lower MP to begin with.
Photon
Member
That's about 125mg/ml.
Thorshammer
Member
Yeah just over a tenth of the volume. In ethanol thats very dilute.
Photon
Member
What do you reckon i get it to?
400mg/ml?
I don't really know the solubility of AAS APIs in ethanol, i'm actually surprised it even holds so well
Thorshammer
Member
You dont want solubility you need ypur product back remember . You need the concentration at about 50 to 60% to crash it out. And thata not full yield but you will get rid of more impurities
Photon
Member
This was 20g, q.s 200ml aka 100mg/ml
pucks looking good
no smell at all
before
after
no smell at all
before
after
Similar threads
