It's still available online (200 proof), but it's pricy.
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https://us.vwr.com/store/catalog/product.jsp?product_id=8920900
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Bradly
Member
Ive made damn near 100% ethanol on my stove top with bread yeast and corn syrup with a tea kettle and some copper tubing.yeah,I know, its a little more involved than that, but its not rocket science either, its second oldest profession I hear. If you already have a distillation setup it should be easy peasy.
use a mineral oil bath to heat your hundred proof to 180 degrees. no open flames. run it through your distillation set up until your satisfied with your product.
use small amounts if your scared you'll blow yourself up. You want to have some real fun, try a good nitration.
use a mineral oil bath to heat your hundred proof to 180 degrees. no open flames. run it through your distillation set up until your satisfied with your product.
use small amounts if your scared you'll blow yourself up. You want to have some real fun, try a good nitration.
Lol . I think the ride across state lines be easierbthan brewing white lightning. You'd still half to distill, just like with hundred proof from liquor store.
It's not that I'm scared I'll blow myself up. I'm scared my wife will use it to set fire to me if I try that in the house : )
Bradly
Member
this is exactly what I did:
http://www.dangerouslaboratories.org/moon1.html
surprised its still up after all these years later. I had to run the alcohol through a couple times to get it to 100% +- . It was good enough for what I needed it for, and you can drink the leftovers
then,well,Walter White would have approved.
http://www.dangerouslaboratories.org/moon1.html
surprised its still up after all these years later. I had to run the alcohol through a couple times to get it to 100% +- . It was good enough for what I needed it for, and you can drink the leftovers
then,well,Walter White would have approved.
^^^ exactly what she would set me on fire for doing!
Bradly
Member
tell her its for the advancement of science,
then apply yourself
then apply yourself
just skimmed this thread and the washing seems pretty simple. Ive used coffee filters for syno and revalor but they clogged easily and were a bitch to work with. Anyone find a better filter set up?
Also, I havent looked much, just a few searches, but would this product work?
http://www.ebay.com/itm/IGNIS-Bio-E...54321455?pt=US_Fireplaces&hash=item3a8bd8732f
Also, I havent looked much, just a few searches, but would this product work?
http://www.ebay.com/itm/IGNIS-Bio-E...54321455?pt=US_Fireplaces&hash=item3a8bd8732f
BIGMESC
New Member
I wouldn't it is denatured with ethyl acetate and denatonium benzonate.
If you are going to use denatured look for one with 90% ethanol 10% methanol.
Just rinse well with distilled water to remove any methanol traces
I think a two stage crystallization is proven to work best. First use your ideal dissolving solvent, ether and others work well..they all have there advantages and disadvantages. Dissolve your product in that solvent . Warm. Filter and evaporate slowly onto your surface of choice. Gather crystals , add to filter and wash with immiscible like water or ethanol wash . One good tip- always presoak your filters to minimize losses.
This will remove more than just washing with your polar solvent.
This will remove more than just washing with your polar solvent.
I think I'll go wander into some dummy source thread --- too many smart people in this thread.
Don't think we have proven anything yet. We don't know if the losses are impurities or hormone yet. I have been meaning to recrystallize the recovered raws from a previous recrystallization to see if the same amount is lost. I just don't have enough raws to play with ATM.
Losses are both hormone and impurities. Also assume maybe the initial reaction during synthesis may not be completely converted. Leaving precursors like androstiene, inert hormones, ect. Your going to lose some in the process even if your in lab environment with magnesium sulfate dried lab grade reagents, but it can be minimized. Its more than worth it Since people have been purifying almost any organic alkaloid this way since chemistry was born . its pretty solid bet that it works here with hormones too. Nothing in science is completely proven. All are hypothesis. But the science literature is there all over the web for those bees that would buzz in those directions.
MANWHORE
Subscriber
The problem is, we don't have access to this testing..
Testing takes time..
Then again, if these underground labs are brewing
in $100,000.00 facilities like they claim, then they
should have testing in that facility
.. Bathtub brew is the way to go...
It's Stylin
Infections are cool
and bathtubs are cheap... unless you get one of those free standing porcelain bitches, then you going to pay, but you ever lay in one of those?? OMG they are to die for
MANWHORE
Subscriber
MANWHORE
Subscriber
I just saved that.. I will read it another time..
M
M
I should have some more in a couple of weeks, but thanks for the offer. I'm keeping a minimal stock because Astro's thread still has me spooked.
I'm also waiting on the results from a couple of other people using different, more advanced extraction methods. The crystals I'm getting from test e don't have the kind of appearance I expected from a pure substance, at least that's my impression from what I've read. Measuring the losses is mostly to verify lack of purification with the method I'm using.
What is your specific procedure? Are you filtering hormone dissolved solvent solution?
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