HPLC RESULT PERFORMED BY AN INDEPENDENT GMP CERTIFIED LAB SIMEC SHOWED PURITY 100.7%!!! Here is the prof!
Everyone who does not believe into this result or thinks that we could change it, can address Simec, provide them individual number of the essay and they confirm it!
Here you find contact data of Simec:
Code:
http://simec.ch/en/ueber-uns/firma.html
Don`t hesitate to contact them by email or phone and ask for confirmation if you have any doubts!
You for sure ask yourself how 100.7% purity is possible? I was also confused yesterday. Today I received explanation which confirmed my assumption.
It is due to the testing technology. I remember the situation when I provided our Internal results for the first time and Dr. JIM criticized me, that testing was done not properly, cause we used not a reference sample as it shall be, but just took data from a database in internet and compared them. So, Simec tested all as it shall be. They bought a reference sample. This is a certified sample of a reference drug. In other words this is ideal drug as it shall be. By the way such sample costs 100 EUR because of certification, etc. And we paid them additionally to get a proper reliable result. After testing this sample by HPLC Simec tested also our sample and compared. Based on comparison is calculated the purity of a drug, how good and bad it is. Reference sample is an ideal drug. This is a sample of proven pharmaceutical grade purity!
I think you all understand what I am going to say… Our sample is by 0.7% purer as certified reference sample! I specially asked Simec about what does it mean and they confirmed it!
I have a very long correspondence with him. Massage is long without it. I will cut and provide only related and essential fragments from different messages of him. If someone doubts whether I changed anything, he can contact me, I provide name and contact data of this specialist and you can copy paste him all text and ask to confirm its authenticity!
A content of 100.7% means, that in relation to the reference substance your sample is a bit more pure (this is not a very strange thing, it happens, depends also on water content of the substances which can vary within a percent, maybe more).
So a content of 100.7% means, that perhaps your sample is very dry (water content less 0.1%), on the other hand the reference standard may contain some tenths of a percent of water. And because the reference standard is named as 100%, the sample is above 100%.
It is not explicit purity - because there may be some impurities which can not be detected with this HPLC-method. It means extended work with determination of linearity, accuracy, recovery, robustness, range, repeatability, precision etc.
Such validations have to be performed for each product separately. Costs for one validation are between 7000 and 15000 EUR (sometimes more, depends very much on the method and sample)
But it is most likely your sample is very pure, a content of >100% really is a very very good result.
As you see this is not absolute pureness. This is pureness based on comparison with a reference drug. Important is that this reference drug is also used to check for quality
pharmaceutical grade products. The reference sample itself is it. Here is what Simec employee said about it:
The reference standard we use is a official certified standard substance, so we can be quite sure, that no relevant impurities are present. Results are calculated with this official standard substance, so there is no doubt that result of content is valid. With a content of 100.7% it is almost evident that there are no impurities in significant amounts.
Nevertheless we cannot make a statement about purity so easy. The content of the sample we determine with an HPLC method which is usable for this substance. But there may be impurities, which cannot be detected with this special method. To be 100% sure, we would have to know all possible impurities and test each of them separately, in worst case each of them with a separate analytical method. There is no global method which can detect all substances at all. And testing for unknown impurities is extremely expensive and time consuming (surely some thousands of EUR or USD).
Ass you have read a full testing in this lab would cost from 7000 to 15000 EUR only for one example. Of course we can not afford this. It is even not needed. First of all cause Simec confirmed that this result is almost evidence, that our sample is pure. In fact, it is a bit purer as the reference sample. Yes, maybe water content, something else. Nevermind. Relevant is that this test has just proven, that at least exactly this batch of nandrolone decanoate is of PHARMACEUTICAL GRADE quality! Yes Pharmacom Labs does not undergo control or certifications from authorized instances, but it absolutely does not mean that we can not produce products of in fact pharmaceutical grade quality.
On top of that this result has just proven that
we have access to pharma grade powder, which some of you did not believe to. Evidence is in this post. I am sure that next results of other raws will continue this positive statistic. We wait for other results. The fun is only beginning…
By the way, almost forgot to mention this. I have already published this result here, but I remind you. This is result performed by our own specialist and at our own chromatograph. This result is not for the current tested batch, but for the previous one. Nevermind. Supplier is the same. Look at it. I know, it is in Chinese, but you can see numbers.
99.409 = 99.4%. The tested sample has in fact 22 substances. One of them is 99.4%. All other 21 substances put together make only 0.6%. They are presented in trace amounts and are by-product. No one compound can be absolutely pure. 99.4% is the absolute value of purity. I remind now how someone criticized me and stated that purity of even 98% is impossible, it would be good if it was at least 95%.... Fuck`em all! 98,5% is minimum what we provide! In case with this and previous deca batch you had in fact pharma grade products! Will see, what other test show…
For those who is interested I can refresh your memory and again provide our internal results, which are great!
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