Qingdao Sigma Chemical Co., Ltd (International, US, EU, Canada and Australia domestic

[Clover 0080]

lol ya forsure u can order drugs on probation forsure the same thing as state laws and not like breaking federal laws on probation... Jesus the brain power here sometimes.

No one is coming to your door over a personal supply of steroids/weightloss drugs, etc. lol

 

[readalot]

I don’t understand your request here, nor the interest.
You’re looking for funding something that has nothing to do with Q samples or have an interest back for my sales, right?

Thanks for running the test and sharing the results. Would be great to drill down on the -ene question in the raw so results aren't diluted by other stuff in the finished product. That's why I am organizing a group buy for an -ene standard so we can run at various ratios with API to determine if the -ene peak is properly resolved from the API peak for Test C and Test E. If it isn't them there are some Test raws on the market that are quite impure. That's what the GCMS testing I had done with a vendor suggests.

 

[Qingdao Sigma Chemicals]

Test Decanoate finished oils results.

An extra GCMS Enhanced testing was added due to suspicions on the quality of raws, tested 90.16% by Deadbeef:

D

Thread 'QSC low purity test decanoate raws'

Dec 28, 2024

Response from Tracy when emailed about it:

Hello, 90% is acceptable. No replacement. Not all batchs will be perfect, some will be +98%, some will be lower, it's the principle of raw powders, so you test them and adjust your brews based on purity results, it's not like if it was contaminated with some other steroid.

• deadbeef
• Replies: 154
• Forum: Analytical Lab Testing

• 
• 

The finished oil was brewed earlier, before his test, assuming the purity is 99%.

The HPLC finished results ended up accurately dosed.



GCMS testing shows no contamination.

The lines 2 and 3 are to be ignore, because it's from Janoshik previous GCMS test of another sample.
17.beta.-Acetoxyandrosta-4,6-dien-3-one is a common impurity found in testosterone raws and other steroids.

The following molecules are MCT constituents:
Glycerol tricaprylate.
2-(Decanoyloxy)propane-1,3-diyl dioctanoate.
3-(Octanoyloxy)propane-1,2-diyl bis(decanoate).
Decanoic acid, 1,2,3-propanetriyl ester.

 

[readalot]

Test Decanoate finished oils results.

An extra GCMS Enhanced testing was added due to suspicions on the quality of raws, tested 90.16% by Deadbeef:

D

Thread 'QSC low purity test decanoate raws'

Dec 28, 2024

Response from Tracy when emailed about it:

Hello, 90% is acceptable. No replacement. Not all batchs will be perfect, some will be +98%, some will be lower, it's the principle of raw powders, so you test them and adjust your brews based on purity results, it's not like if it was contaminated with some other steroid.

• deadbeef
• Replies: 154
• Forum: Analytical Lab Testing

• 
• 

The finished oil was brewed earlier, before his test, assuming the purity is 99%.

The HPLC finished results ended up accurately dosed.

View attachment 310984

GCMS testing shows no contamination.

The lines 2 and 3 are to be ignore, because it's from Janoshik previous GCMS test of another sample.
17.beta.-Acetoxyandrosta-4,6-dien-3-one is a common impurity found in testosterone raws and other steroids.

The following molecules are MCT constituents:
Glycerol tricaprylate.
2-(Decanoyloxy)propane-1,3-diyl dioctanoate.
3-(Octanoyloxy)propane-1,2-diyl bis(decanoate).
Decanoic acid, 1,2,3-propanetriyl ester.

View attachment 310989
View attachment 310990
View attachment 310991
View attachment 310992

To confirm, that's GCMS of finished oil. Well done. Testing the raws with GCMS even more useful (no dilution with other stuff you add to make finished product).

Very useful tool. Now we need to put the question on Test C and Test E raws to bed. That's where the reference standard for -ene impurity becomes critical. Will allow determination if that impurity is "invisible" to HPLC (vs API).

 

[Cereal masturbator]

Test Decanoate finished oils results.

An extra GCMS Enhanced testing was added due to suspicions on the quality of raws, tested 90.16% by Deadbeef:

D

Thread 'QSC low purity test decanoate raws'

Dec 28, 2024

Response from Tracy when emailed about it:

Hello, 90% is acceptable. No replacement. Not all batchs will be perfect, some will be +98%, some will be lower, it's the principle of raw powders, so you test them and adjust your brews based on purity results, it's not like if it was contaminated with some other steroid.

• deadbeef
• Replies: 154
• Forum: Analytical Lab Testing

• 
• 

The finished oil was brewed earlier, before his test, assuming the purity is 99%.

The HPLC finished results ended up accurately dosed.

View attachment 310984

GCMS testing shows no contamination.

The lines 2 and 3 are to be ignore, because it's from Janoshik previous GCMS test of another sample.
17.beta.-Acetoxyandrosta-4,6-dien-3-one is a common impurity found in testosterone raws and other steroids.

The following molecules are MCT constituents:
Glycerol tricaprylate.
2-(Decanoyloxy)propane-1,3-diyl dioctanoate.
3-(Octanoyloxy)propane-1,2-diyl bis(decanoate).
Decanoic acid, 1,2,3-propanetriyl ester.

View attachment 310989
View attachment 310990
View attachment 310991
View attachment 310992

I used to leave cash in someone’s bag in the gym and he’d drop the gear In my bag in the changing room, now we get whatever the fuck these graphs are with our order …. As bob Dylan wrote, the times they are a changing

 

[readalot]

I used to leave cash in someone’s bag in the gym and he’d drop the gear In my bag in the changing room, now we get whatever the fuck these graphs are with our order …. As bob Dylan wrote, the times they are a changing

You are welcome.

 

[Qingdao Sigma Chemicals]

To confirm, that's GCMS of finished oil. Well done. Testing the raws with GCMS even more useful (no dilution with other stuff you add to make finished product).

Very useful tool. Now we need to put the question on Test C and Test E raws to bed. That's where the reference standard for -ene impurity becomes critical. Will allow determination if that impurity is "invisible" to HPLC (vs API).

Good luck with that.
QSC will always continue to perform whatever testing is need to advertise its products, and whenever there is an interest that brings a return of investment.
I am sure when the interest in your question one day raises, you'll see more participants in the subject.

 

[MyNameIsJeff]

Test Decanoate finished oils results.

An extra GCMS Enhanced testing was added due to suspicions on the quality of raws, tested 90.16% by Deadbeef:

D

Thread 'QSC low purity test decanoate raws'

Dec 28, 2024

Response from Tracy when emailed about it:

Hello, 90% is acceptable. No replacement. Not all batchs will be perfect, some will be +98%, some will be lower, it's the principle of raw powders, so you test them and adjust your brews based on purity results, it's not like if it was contaminated with some other steroid.

• deadbeef
• Replies: 154
• Forum: Analytical Lab Testing

• 
• 

The finished oil was brewed earlier, before his test, assuming the purity is 99%.

The HPLC finished results ended up accurately dosed.

View attachment 310984

GCMS testing shows no contamination.

The lines 2 and 3 are to be ignore, because it's from Janoshik previous GCMS test of another sample.
17.beta.-Acetoxyandrosta-4,6-dien-3-one is a common impurity found in testosterone raws and other steroids.

The following molecules are MCT constituents:
Glycerol tricaprylate.
2-(Decanoyloxy)propane-1,3-diyl dioctanoate.
3-(Octanoyloxy)propane-1,2-diyl bis(decanoate).
Decanoic acid, 1,2,3-propanetriyl ester.

View attachment 310989
View attachment 310990
View attachment 310991
View attachment 310992

I don't understand.

Either

- the HPLC test of the raws (90% purity) is correct

Or

- The GCMS test of the oil (no impurities corresponding to the 10% of the weight of the raws detected) is correct

I do not see how both tests could be correct. Unless the impurity detected in the HPLC somehow disappeared in the brewing process (like water evaporating).

Help a brotha out here

 

[readalot]

I don't understand.

Either

- the HPLC test of the raws (90% purity) is correct

Or

- The GCMS test of the oil (no impurities corresponding to the 10% of the weight of the raws detected) is correct

I do not see how both tests could be correct. Unless the impurity detected in the HPLC somehow disappeared in the brewing process (like water evaporating).

Help a brotha out here

Finally getting some interest in this important topic. I will be reading with keen enjoyment. Thanks for asking the questions.

Lots of degrees of freedom in there to nail the answers down.

 

[AlmightyAlpha]

Good luck with that.
QSC will always continue to perform whatever testing is need to advertise its products, and whenever there is an interest that brings a return of investment.
I am sure when the interest in your question one day raises, you'll see more participants in the subject.

Bunch of my 12/19 packs are clearing and landing. Thank you.

 

[VakarianSK]

would you guys consider this lost or does Uni just suck this much

No, I had the same situation. If it's delivered to local Carrier you are fine. Mine was delivered to the local Carrier for over two weeks with no change and then it finally got an update and started moving on day 15 or 16.

 

[Qingdao Sigma Chemicals]

I don't understand.

Either

- the HPLC test of the raws (90% purity) is correct

Or

- The GCMS test of the oil (no impurities corresponding to the 10% of the weight of the raws detected) is correct

I do not see how both tests could be correct. Unless the impurity detected in the HPLC somehow disappeared in the brewing process (like water evaporating).

Help a brotha out here

We performed both HPLC and GCMS testing on the Test D oil here.

No impurity was reflected on the oil sample, despite using the same batch for making oils.

The only explanations possible:
- test D finished oil is overdosed.
- the test D raw sample was not correctly handled by the buyer, which resulted in the lower purity results.

Only an extra test D raw testing from someone else who purchased the test D raws can confirm, and ideally if he includes the GCMS test.

 

[Sampei]

I don't understand.

Either

- the HPLC test of the raws (90% purity) is correct

Or

- The GCMS test of the oil (no impurities corresponding to the 10% of the weight of the raws detected) is correct

I do not see how both tests could be correct. Unless the impurity detected in the HPLC somehow disappeared in the brewing process (like water evaporating).

Help a brotha out here

I was thinking the same, if the brew was done with 99% purity in mind the oil should come underdosed by at least 9/10%

 

[Sampei]

We performed both HPLC and GCMS testing on the Test D oil here.

No impurity was reflected on the oil sample, despite using the same batch for making oils.

The only explanations possible:
- test D finished oil is overdosed.
- the test D raw sample was not correctly handled by the buyer, which resulted in the lower purity results.

Only an extra test D raw testing from someone else who purchased the test D raws can confirm, and ideally if he includes the GCMS test.

I'll have to be that guy, would you like to help me out Tracy? Not saying you should fund the whole test (even so it would be appreciated) but a contribution would be appreciated

 

[bighunanballs]

@Qingdao Sigma Chemicals you guys gonna synthesize NA-931 soon?

NA-931

NA-931 is for the treatment Diabetes Obesity and Alcohol Use Disorder

www.biomedind.com

 

[Qingdao Sigma Chemicals]

I'll have to be that guy, would you like to help me out Tracy? Not saying you should fund the whole test (even so it would be appreciated) but a contribution would be appreciated

Sure and ideally send it in optimum conditions to eliminate any possible contamination/impurity scenario from air and humidity.
Mylar bag + silica packet
Like Rido testing on oxy, I can contribute to a part of it:

Thread 'Analysis of Anadrol powder'

Oct 3, 2023

So as some of you know. I was getting irritated with my Anadrol capsule making, it was 20% overdosed. Also some of the test reports havent been great.

I have made 3 sets of capsules and tried to fix my recipe. all have been overdosed. Last time was only 10% overdosed when I decided not to intentionally not make up for the lack of purity. This is when I was questioning if the filler and mixing process was drying out the water from the anadrol?

Some of those that do not know about Anadrol is that it is flour like. I was suspecting water content could play a role. At the same time some...

• Rido
• Replies: 12
• Forum: Analytical Lab Testing

• 
• 

 

[Qingdao Sigma Chemicals]

@Qingdao Sigma Chemicals you guys gonna synthesize NA-931 soon?

NA-931

NA-931 is for the treatment Diabetes Obesity and Alcohol Use Disorder

www.biomedind.com

We don’t synthesize anything beside HGH and IGF.
If some interest is there in the market we will be able to purchase some and sell it, first time to hear about it.

 

[Sampei]

Sure and ideally send it in optimum conditions to eliminate any possible contamination/impurity scenario from air and humidity.
Mylar bag + silica packet
Like Rido testing on oxy, I can contribute to a part of it:

Thread 'Analysis of Anadrol powder'

Oct 3, 2023

So as some of you know. I was getting irritated with my Anadrol capsule making, it was 20% overdosed. Also some of the test reports havent been great.

I have made 3 sets of capsules and tried to fix my recipe. all have been overdosed. Last time was only 10% overdosed when I decided not to intentionally not make up for the lack of purity. This is when I was questioning if the filler and mixing process was drying out the water from the anadrol?

Some of those that do not know about Anadrol is that it is flour like. I was suspecting water content could play a role. At the same time some...

• Rido
• Replies: 12
• Forum: Analytical Lab Testing

• 
• 

The sample is inside a small sealed plastic vial kept in a dark dry place at the moment. Would you find it acceptable? That's usually how I send all my raw sample.

 

[Sampei]

We don’t synthesize anything beside HGH and IGF.
If some interest is there in the market we will be able to purchase some and sell it, first time to hear about it.

Is it possible to synthetize real IGF-1 same as increlex so no L3 or Des?

 

[Qingdao Sigma Chemicals]

The sample is inside a small sealed plastic vial kept in a dark dry place at the moment. Would you find it acceptable? That's usually how I send all my raw sample.

Add silica packet, to absord humidity. Elimnate every doubt.