HPLC/MS Analysis on Various Substances *RESULTS*

[Capt Forest]

I got a response saying he will have them done april 1st or shortly after. Sorry for the wait. And my absence from the community

 

[Mr.B66]

Cool cap, looking forward to those clomid and adex results!!!

 

[WMSuperSport]

Why did Dr. Jim's post just get removed?

 

[Millard]

Why did Dr. Jim's post just get removed?

He deleted it.

 

[WMSuperSport]

damn, i liked it

 

[Dr JIM]

He deleted it.

One of those Meso minions did it again Millard!

 

[Dr JIM]

Yea I deleted it AND moved it to "Jim's HPLC" thread.

So you can still "like it" and let me know your preference there fella

 

[iMONSTERoid]

Here is a key so that you will know which sample corresponds to what product i sent in. Some of the samples are not public and i was never made aware of the brand so i am not able to list it. But the analysis will be up for viewing.

Sample 1 - Legend Anavar lot 201404025
Sample 2 - Legend Anavar lot 201407025
Sample 3 - Purity Source labs Anavar
Sample 4 - Swole oil Anavar (10mg pill)
Sample 5 - Legend Clomid (GKH)
Sample 6 - Test enanthate
Sample 7 - World Pharma Test prop
Sample 8 - Test prop
Sample 9 - MJR Caber
Sample 10 - Maximum Peptide T3
Sample 11 - MJR t3/t4 combo
Sample 12 - MJR Exemestane


Here is a slide by slide walk walk through that the scientist who performed the analysis gave me. Its a 19 page report.

"The pdf of the powerpoint slides has the chromatograms for the mass spec runs (examples). I will walk you through those: The first slide shows injections of Testosterone and Oxandrolone Standards, eluting at ~17 min. Slide 2 shows the chromatograms for samples 1 to 4, showing the expected peaks for oxandrolone for each sample. I prepared 2 replicate samples for each sample that you provided. Slide 3 shows the results for Clomiphene citrate. Samples 1 to 5 were triturated and extracted into chloroform or ethyl acetate/methanol (for sample 5) to extract the active compounds. For samples 6 to 12 I diluted them about 100 fold into ethyl acetate. Slides 4 and 5 show the results for Sample 6A and 6B. The main component is the enanthate, but there is a bit of the propionate which is hard to quantitate, and some testosterone, also in small amounts. I can send the HPLC chromatography for samples 6 to 8 if you are interested in seeing the absorption peaks. Slides 6 to 9 show the chromatograms for samples 7A, 7B, 8A and 8B. Notice that there is some "free" testosterone in these samples, also hard to quantify, and that the peak for the propionate does produce some testosterone in the spectrometer, which has no effect on the analysis. Slides 10 and 11 are for sample 9, showing NO cabergoline present, but some exemestane is observed and it was quantificated, based on the external calibration curve. The slides number 12 to 15 show that there is not much T3 or T4 (thyroxine) in samples10 and 11, but still could be quantified. I did notice that T4 tends to degrade into T3 from my standards, but those were prepared in water solutions, unlike the samples that you sent which should be more stable. Slides 16 and 17 are for the exemestane sample, it is present as the main component in large amounts in sample 12.

Finally slide 18 shows the summary of the HPLC quantification for samples 6 to 8, using HPLC with UV detection with testosterone as a standard. I performed 2 injections for each sample and 2 dilutions for each sample. I had to repeat sample 6 as one of the dilutions showed too much compound (6B) for some reason, and which should be neglected. The elution times agree with the LC-MS results, so the peaks were assigned according to what I observed in those chromatograms. The final numbers are shown in yellow. The last slide has the summary of all the results in the last column shown in pink. For the tablets the results are total mg per tablet, while for the liquid samples they are shown in mg/mL."

This was the first batch of tests ran. There is another in the works atm. If anyone is interseted in having anything tested send me a pm. Here is a list of items i have refrence standards for from sigma alderich. I can only test items on this list. With out a refrence standard labs like this are usless.
Testosterone
Oxandrolone
Exemestane
Clomiphene Citrate
Cabergoline
Triiodothyronine
Thyroxine
Anastrozole

I would like to get more RC chems checked out that way we can as a community narrow down some good stuff. As you can see MJR fucked me on the caber and asin but came through on the t3.

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PS. I am aware that the scientist spelled oxandrolone wrong in the reports.

Great work Capt

 

[Capt Forest]

I sent for an update i will relay it when i comes

 

[Capt Forest]

UPDATE:

http://prntscr.com/6phtpl

 

[Burrr]

you teasing us bro?

 

[WMSuperSport]

Haha, that was a damn tease. I fell for it.

 

[WMSuperSport]

My TT bw came back at 10x, so lets see what these next round of these tests show. I'm pretty damn boned up about it.

 

[Capt Forest]

I have no clue what the hold up is. sorry this is taking 5 ever

 

[WMSuperSport]

lol its all good. who knows. maybe he got caught up in some poo-nani

 

[flenser]

@Capt Forest do you know if he is still taking samples (and payment)? This is starting to feel like Angus, or Astro's Chinese lab, or two others I paid to have samples tested and never got anything back. 12 weeks is a long time to wait. I worry he's still collecting payment and no longer testing.

 

[romaleos]

Sample 8 is Ultimate Pharmaceuticals. Bloods to follow on Monday.

 

[Capt Forest]

its nothing like the angus situation. I have 100% confidance this will get finished with the same quality presentation as the last batch.

I will send for an update

 

[flenser]

its nothing like the angus situation. I have 100% confidance this will get finished with the same quality presentation as the last batch.

I will send for an update

I hope you are right. I don't mind the wait so much as the uncertainty. My track record with labs is worse than than it is with gear, a lot worse.

 

[Capt Forest]

I hope you are right. I don't mind the wait so much as the uncertainty. My track record with labs is worse than than it is with gear, a lot worse.

I Am honestly surprised with the level of patience and respect everyone involved with this batch has shown me. Thanks for that. I expected to be burned at the stake by now.